Crystal structure of ethyl 2-[2-((1E)-{(1E)-2-[2-(2-ethoxy-2-oxoethoxy)benzyl-idene]hydrazin-1-ylidene}methyl)phen-oxy]acetate

Joel T. Mague; Shaaban K. Mohamed; Mehmet Akkurt; Eman A. Ahmed; Omran A. Omran; W. T A Harrison

doi:10.1107/S2056989014025584

Crystal structure of ethyl 2-[2-((1E)-{(1E)-2-[2-(2-ethoxy-2-oxoethoxy)benzyl-idene]hydrazin-1-ylidene}methyl)phen-oxy]acetate

Joel T. Mague
, Shaaban K. Mohamed
, Mehmet Akkurt
, Eman A. Ahmed^*
, Omran A. Omran
, W. T A Harrison (Editor)

^*Corresponding author for this work

Chemistry

Tulane University
Minia University
Erciyes University
Sohag University

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

9 Downloads (Pure)

Abstract

The complete molecule of the title compound, C2₂H₂4N₂O₆, is generated by crystallographic inversion symmetry and is approximately planar (r.m.s. deviation of the non-H atoms = 0.134 A). The packing consists of inter-digitated sheets inclined at 25.9 (4)° to one another and linked by short C - H⋯O hydrogen bonds.

Original language	English
Pages (from-to)	o16
Number of pages	1
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	71
Issue number	1
DOIs	https://doi.org/10.1107/S2056989014025584
Publication status	Published - 1 Jan 2015

Bibliographical note

NSF–MRI grant No. 1228232 for the purchase of the diffractometer and Tulane University for support of the Tulane Crystallography Laboratory are gratefully acknowledged.

Keywords

Azomethenes
Bis-phenoxy carboxylate
Crystal structure

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10.1107/S2056989014025584Licence: CC BY

Crystal structure of ethyl 2-[2-((1E)-{(1E)-2-[2-(2-ethoxy-2-oxoethoxy)benzylidene]hydrazin-1-ylidene}methyl)phenoxy]acetate
© 2015 Magueet al. Licence: Creative Commons Attribution (CC-BY)
Final published version, 287 KBLicence: CC BY

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title = "Crystal structure of ethyl 2-[2-((1E)-\{(1E)-2-[2-(2-ethoxy-2-oxoethoxy)benzyl-idene]hydrazin-1-ylidene\}methyl)phen-oxy]acetate",

abstract = "The complete molecule of the title compound, C22H24N2O6, is generated by crystallographic inversion symmetry and is approximately planar (r.m.s. deviation of the non-H atoms = 0.134 A). The packing consists of inter-digitated sheets inclined at 25.9 (4)° to one another and linked by short C - H⋯O hydrogen bonds.",

keywords = "Azomethenes, Bis-phenoxy carboxylate, Crystal structure",

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note = "NSF{\textendash}MRI grant No. 1228232 for the purchase of the diffractometer and Tulane University for support of the Tulane Crystallography Laboratory are gratefully acknowledged.",

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doi = "10.1107/S2056989014025584",

language = "English",

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T1 - Crystal structure of ethyl 2-[2-((1E)-{(1E)-2-[2-(2-ethoxy-2-oxoethoxy)benzyl-idene]hydrazin-1-ylidene}methyl)phen-oxy]acetate

AU - Mague, Joel T.

AU - Mohamed, Shaaban K.

AU - Akkurt, Mehmet

AU - Ahmed, Eman A.

AU - Omran, Omran A.

A2 - Harrison, W. T A

N1 - NSF–MRI grant No. 1228232 for the purchase of the diffractometer and Tulane University for support of the Tulane Crystallography Laboratory are gratefully acknowledged.

PY - 2015/1/1

Y1 - 2015/1/1

N2 - The complete molecule of the title compound, C22H24N2O6, is generated by crystallographic inversion symmetry and is approximately planar (r.m.s. deviation of the non-H atoms = 0.134 A). The packing consists of inter-digitated sheets inclined at 25.9 (4)° to one another and linked by short C - H⋯O hydrogen bonds.

AB - The complete molecule of the title compound, C22H24N2O6, is generated by crystallographic inversion symmetry and is approximately planar (r.m.s. deviation of the non-H atoms = 0.134 A). The packing consists of inter-digitated sheets inclined at 25.9 (4)° to one another and linked by short C - H⋯O hydrogen bonds.

KW - Azomethenes

KW - Bis-phenoxy carboxylate

KW - Crystal structure

UR - https://www.scopus.com/pages/publications/84928154084

U2 - 10.1107/S2056989014025584

DO - 10.1107/S2056989014025584

M3 - Article

AN - SCOPUS:84928154084

SN - 1600-5368

VL - 71

SP - o16

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 1

ER -

Crystal structure of ethyl 2-[2-((1E)-{(1E)-2-[2-(2-ethoxy-2-oxoethoxy)benzyl-idene]hydrazin-1-ylidene}methyl)phen-oxy]acetate

Abstract

Bibliographical note

Keywords

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