Synthesis and analysis by liquid chromatography-mass spectrometry of a mauveine composition similar to museum-stored mauveine

Michael J. Plater; Andrea Raab

doi:10.3184/174751918X15411642455207

Synthesis and analysis by liquid chromatography-mass spectrometry of a mauveine composition similar to museum-stored mauveine

Michael J. Plater^* (Corresponding Author), Andrea Raab

^*Corresponding author for this work

Chemistry

Research output: Contribution to journal › Article › peer-review

7 Citations (Scopus)

22 Downloads (Pure)

Abstract

Our proposal that museum stored mauveine was made by a modified method compared to mauveine made by the William Henry Perkin (WHP) patented method of 1856 is exemplified. An improved method of purification allows greater resolution and separation of the different mauveine chromophores. LC-MS charts for museum stored mauveine are compared to the new mauveine reported here. The formation of deprotected mauveine chromophores and N-tert-butylated mauveine chromophores is discussed.

Original language	English
Pages (from-to)	589-594
Number of pages	6
Journal	Journal of Chemical Research
Volume	42
Issue number	12
Early online date	22 Nov 2018
DOIs	https://doi.org/10.3184/174751918X15411642455207
Publication status	Published - Dec 2018

Bibliographical note

We are grateful to the EPSRC National Mass Spectrometry Foundation (NMSF) for mass spectra.

Keywords

mauve
mauveine
liquid chromatography-mass spectrometry
silica gel

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10.3184/174751918X15411642455207Licence: Unspecified

Accepted Manuscript
This is an Accepted Manuscript of an article published by Science Reviews 2000 Ltd in Journal of Chemical Research on 22 Nov 2018, available online: https://stl.publisher.ingentaconnect.com/contentone/stl/jcr/2018/00000042/00000012/art00001
Accepted author manuscript, 726 KBLicence: Unspecified
Supplementary InformationAccepted author manuscript, 783 KBLicence: Unspecified

Cite this

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abstract = "Our proposal that museum stored mauveine was made by a modified method compared to mauveine made by the William Henry Perkin (WHP) patented method of 1856 is exemplified. An improved method of purification allows greater resolution and separation of the different mauveine chromophores. LC-MS charts for museum stored mauveine are compared to the new mauveine reported here. The formation of deprotected mauveine chromophores and N-tert-butylated mauveine chromophores is discussed.",

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AU - Plater, Michael J.

AU - Raab, Andrea

N1 - We are grateful to the EPSRC National Mass Spectrometry Foundation (NMSF) for mass spectra.

PY - 2018/12

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N2 - Our proposal that museum stored mauveine was made by a modified method compared to mauveine made by the William Henry Perkin (WHP) patented method of 1856 is exemplified. An improved method of purification allows greater resolution and separation of the different mauveine chromophores. LC-MS charts for museum stored mauveine are compared to the new mauveine reported here. The formation of deprotected mauveine chromophores and N-tert-butylated mauveine chromophores is discussed.

AB - Our proposal that museum stored mauveine was made by a modified method compared to mauveine made by the William Henry Perkin (WHP) patented method of 1856 is exemplified. An improved method of purification allows greater resolution and separation of the different mauveine chromophores. LC-MS charts for museum stored mauveine are compared to the new mauveine reported here. The formation of deprotected mauveine chromophores and N-tert-butylated mauveine chromophores is discussed.

KW - mauve

KW - mauveine

KW - liquid chromatography-mass spectrometry

KW - silica gel

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DO - 10.3184/174751918X15411642455207

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JF - Journal of Chemical Research

IS - 12

ER -

Synthesis and analysis by liquid chromatography-mass spectrometry of a mauveine composition similar to museum-stored mauveine

Abstract

Bibliographical note

Keywords

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Cite this